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RSS FeedsSelective and reversible 1,3-dipolar cycloaddition of 6-aryl-1,5-diazabicyclo[3.1.0]hexanes with 1,3-diphenylprop-2-en-1-ones under microwave irradiation (Beilstein Journal of Organic Chemistry)

 
 

30 october 2020 10:47:16

 
Selective and reversible 1,3-dipolar cycloaddition of 6-aryl-1,5-diazabicyclo[3.1.0]hexanes with 1,3-diphenylprop-2-en-1-ones under microwave irradiation (Beilstein Journal of Organic Chemistry)
 


Abstract The first example of the cycloaddition of in situ-generated azomethine imine under microwave conditions is described. The reaction of 6-aryl-1,5-diazabicyclo[3.1.0]hexanes with 1,3-diphenylprop-2-en-1-ones proceeds regio- and stereoselectively giving mostly good yields of the corresponding perhydropyrazolopyrazoles. The products of the reaction undergo cycloreversion under the reaction conditions. Beilstein J. Org. Chem. 2020, 16, 2679–2686. doi:10.3762/bjoc.16.218


 
207 viewsCategory: Chemistry
 
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