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22 january 2021 10:17:23

Total synthesis of decarboxyaltenusin (Beilstein Journal of Organic Chemistry)

Abstract The total synthesis of decarboxyaltenusin (5’-methoxy-6-methyl-[1,1’-biphenyl]-3,3’,4-triol), a toxin produced by various mold fungi, has been achieved in seven steps in a yield of 31% starting from 4-methylcatechol and 1-bromo-3,5-dimethoxybenzene, where the longest linear sequence consists of five steps. The key reaction was a palladium-catalyzed Suzuki coupling of an aromatic boronate with a brominated resorcin derivative. Beilstein J. Org. Chem. 2021, 17, 224–228. doi:10.3762/bjoc.17.22

60 viewsCategory: Chemistry
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