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RSS FeedsMolbank, Vol. 2019, Article M1061: 4b,5,6,9-Tetrahydro-7H-dibenzo[c,e]pyrrolo[1,2-a]azepin-7-one (Molbank)

 
 

17 may 2019 21:03:28

 
Molbank, Vol. 2019, Article M1061: 4b,5,6,9-Tetrahydro-7H-dibenzo[c,e]pyrrolo[1,2-a]azepin-7-one (Molbank)
 




A simple approach to synthesize 4b,5,6,9-tetrahydro-7H-dibenzo[c,e]pyrrolo[1,2-a]azepin- 7-one has been developed, based on a three-step transformation of 2-(2-bromophenyl)cyclopropane-1,1-diester. The key stage in this method is an intramolecular cross-coupling of 1-(2-bromobenzyl)-5-(2-bromophenyl)pyrrolidin-2-one under continuous flow conditions in an H-?ube-Pro using commercially available supported Pd catalysts.


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27 viewsCategory: Biochemistry, Chemistry, Molecular Biology
 
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